Page 210 - Дисертація_Влад_Христина_Ігорівна

Рентгенівська фотоелектронна спектроскопія

Ni Pd -R
90
10
None None
80
20 Name Pos. FWHM Area At% Name Pos. FWHM L.Sh. Area %Area
O 1s 531.36 4.98 188098.85 48.68 None 530.92 2.61 GL(30) 121338.36 65.22
18 C 1s 284.36 4.78 48348.88 36.66 None 533.59 2.79 GL(30) 54095.78 29.08
Na 1s 1072.36 4.93 10167.55 0.90 70 None 528.77 1.59 GL(30) 10600.82 5.70
Ni 2p 855.36 9.07 334633.26 11.43
16
Pd 3d 334.36 8.25 24172.54 1.15
Fe 2p 711.36 5.79 25458.09 1.18 60
Pos. FWHM
Area
At%
14 Name 530.97 3.76 185848.81 100.00
CPS x 10 -4 12 CPS x 10 -3 50
O 1s
10
8 40
6
30
4
2 20
1000 800 600 400 200 0 550 545 540 535 530 525 520 515
Binding Energy (eV) Binding Energy (eV)
1
а
CasaXPS (This string can be edited in CasaXPS.DEF/PrintFootNote.txt) CasaXPS (This string can be edited in CasaXPS.DEF/PrintFootNote.txt)
None None
80
Name Pos. FWHM L.Sh. Area %Area Name Pos. FWHM L.Sh. Area %Area
None 855.51 3.26 GL(30) 412424.03 25.05 95 None 336.22 3.18 GL(30) 35450.55 31.86
75 None 875.32 3.88 GL(30) 126959.22 7.71 None 334.30 1.80 GL(30) 31631.04 28.43
None 880.10 6.24 GL(30) 310175.28 18.84 90 None 339.63 1.98 GL(30) 24974.03 22.44
None 861.55 6.67 GL(30) 479744.74 29.14 None 341.79 2.85 GL(30) 19217.15 17.27
70 None 851.89 2.02 GL(30) 30356.43 1.84
None 857.85 2.66 LA(1,643) 115707.04 10.40 85
7.03
CPS x 10 -4 65 Name 855.57 5.65 1639937.23 100.00 CPS x 10 -3 80 Name 334.57 3.19 110925.68 100.00
171211.72
3.37
873.07
None
LA(1,643)
Pos. FWHM
Area
At%
Pd 3d
Pos. FWHM
Area
At%
Ni 2p
60
75
55
70
50
65
45
60
890 880 870 860 850 840 348 344 340 336 332 328
Binding Energy (eV) Binding Energy (eV)
2 3
CasaXPS (This string can be edited in CasaXPS.DEF/PrintFootNote.txt) CasaXPS (This string can be edited in CasaXPS.DEF/PrintFootNote.txt)
Co-R
None
14 Name Pos. FWHM Area At%
O 1s 534.39 4.09 188041.17 53.39
C 1s 288.39 7.29 38302.65 31.86
12 Co 2p 783.39 5.23 340300.94 14.74
10
CPS x 10 -4 8
6
4
2
1000 800 600 400 200 0

Binding Energy (eV)
б
CasaXPS (This string can be edited in CasaXPS.DEF/PrintFootNote.txt)

208